Ipzz-266 !full! »

Polymer A was obtained by coupling Monomer 1 (5 mmol) with 2,5‑bis(pinacolborane)‑3‑hexylthiophene (5 mmol) using Pd(OAc)₂ (0.05 mmol) and TFP (0.10 mmol) in a 1:1 mixture of THF/DMF (100 mL) with K₂CO₃ (10 mmol) as base. The reaction proceeded at 90 °C for 48 h under N₂. After work‑up and precipitation into methanol, Gel‑Permeation Chromatography (GPC, THF, polystyrene standards) indicated Mₙ = 28 kDa, Đ ≈ 1.12.

Thin films (≈ 15 µm) of IPZZ‑266 were spin‑coated onto a pre‑stretched silicone elastomer (Ecoflex 00‑30) and cured at 70 °C for 30 min. Electrical contacts were defined by sputtering gold pads (50 nm) through a shadow mask. IPZZ-266

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